Advanced practical organic chemistry by Leonard, John; Lygo, B.; Procter, Garry

By Leonard, John; Lygo, B.; Procter, Garry

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Dated spectra and other analytical data to complement the experiment also add weight to its validity. When an ELN is used to record experiments, the records should be captured in a version controlled relational database that is maintained and validated for the capture of electronic records and signatures. When a document is saved in this type of database, the time and date are permanently associated with it and the version is also saved indelibly. Any versions subsequently saved are kept, in addition to previous ones, to provide an audit trail.

UV-vis, optical rotatory dispersion, and circular dichroism). Your supervisor should be able to advise on which additional types of data are appropriate. 3 Organizing your data records It is essential that you organize your data records in a way that allows you to link a piece of data to the experiment that generated it and also allows you to rapidly locate all the data for a particular compound. There are various ways of doing this and your supervisor should be able to advise on the most appropriate method.

Fraudulent results have been reported from time to time and there can be disputes over originality or plagiarism, so having evidence of when an experiment was carried out is always of the utmost importance. For paper notebook experimental records, every experiment should be dated at the start and signed and dated when finished. In many laboratories, countersignatures are required, where a colleague signs and dates the experiment, and this may add some value if the authenticity of the experiment is questioned.

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